Influence of Interpass Welding Temperature on the Microstructure and Mechanical Properties of Super Duplex Stainless Steel AISI 2507

Authors

  • Mohammed Helan Sar Department of Applied Mechanics Techniques Engineering, Engineering Technical College, Middle Technical University, Baghdad, Iraq
  • Sara H. Shahatha Department of Materials Techniques Engineering, Engineering Technical College, Middle Technical University, Baghdad, Iraq
  • Sami Chatti Laboratory of Mechanical Engineering, National Engineering School of Monastir, University of Monastir, Tunisia
  • Mondher Zidi Laboratory of Mechanical Engineering, National Engineering School of Monastir, University of Monastir, Tunisia

DOI:

https://doi.org/10.24237/djes.2026.19212

Keywords:

Stainless steel AISI2507 , ER2209, GTAW, cooling rate, temperature, Multipass welding

Abstract

This study investigates the combined influence of interpass temperature and cooling rate on the microstructure and mechanical properties of 10-mmthick AISI 2507 superduplex stainless steel welded by multi-pass gas tungsten arc welding (GTAW) using ER2209 filler metal. Welded joints were produced under controlled thermal conditions to evaluate the effect of welding thermal cycles on phase evolution and hardness distribution. Optical microscopy, X-ray diffraction (XRD), and Vickers microhardness testing were employed to characterize the weld metal (WM), heat-affected zone (HAZ), and base metal (BM). The results demonstrated that cooling rate was the dominant parameter governing microstructural evolution. Rapid cooling promoted the formation of a finer duplex microstructure with a more homogeneous ferrite–austenite distribution, whereas slower cooling resulted in grain coarsening and increased ferrite retention at grain boundaries. The investigated interpass temperature range (150–350°C) had only a limited influence on the mechanical response, with the weld metal hardness remaining nearly constant at approximately 288–289 HV, indicating that the ferrite–austenite balance was effectively maintained under the selected welding conditions. XRD analysis confirmed the preservation of the duplex structure through the characteristic ferrite (α) (110) and (200) and austenite (γ) (111) and (200) diffraction peaks in all welded samples. However, the slower-cooling condition exhibited higher ferrite peak intensities, suggesting reduced austenite reformation during solidification. The combined microstructural, XRD, and hardness results demonstrate that the cooling rate exerts a greater influence than the interpass temperature on phase stability, microstructural refinement, and the overall metallurgical performance of multi-pass GTAW AISI 2507.

Downloads

Download data is not yet available.

References

[1] K. W. Chan and S. C. Tjong, “Effect of secondary phase precipitation on the corrosion behavior of duplex stainless steels,” Materials, vol. 7, no. 7, pp. 5268–5304, 2014, doi: 10.3390/ma7075268.

[2] A. K. Maurya, C. Pandey, and R. Chhibber, “Dissimilar welding of duplex stainless steel with Ni alloys: A review,” International Journal of Pressure Vessels and Piping, vol. 192, Art. no. 104439, 2021, doi: 10.1016/j.ijpvp.2021.104439.

[3] H. Wang, A. Wang, C. Li, X. Yu, J. Xie, and C. Liu, “Effect of secondary-phase precipitation on mechanical properties and corrosion resistance of 00Cr27Ni7Mo5N hyper-duplex stainless steel during solution treatment,” Materials, vol. 15, no. 21, Art. no. 7533, 2022, doi: 10.3390/ma15217533.

[4] Y. Peng, Y. Du, Y. Zhang, W. Ma, and Q. Liang, “Effect of solution treatment on microstructure and mechanical properties of laser-cladded Stellite 6 coatings on 2507 duplex stainless steel,” Materials Today Communications, vol. 46, Art. no. 112795, 2025, doi: 10.1016/j.mtcomm.2025.112795.

[5] L. Chen, H. Tan, Z. Wang, J. Li, and Y. Jiang, “Influence of cooling rate on microstructure evolution and pitting corrosion resistance in the simulated heat-affected zone of 2304 duplex stainless steels,” Corrosion Science, vol. 58, pp. 168–174, 2012, https://doi.org/10.1016/j.corsci.2012.01.018.

[6] G. Chagas de Souza et al., “Mechanical properties and corrosion resistance evaluation of superduplex stainless steel UNS S32760 repaired by GTAW process,” Welding International, vol. 30, no. 6, pp. 432–442, 2016, doi: 10.1080/09507116.2015.1096527.

[7] O. S. Barrak, S. Ben-Elechi, and S. Chatti, “Parameters influence on mechanical properties of resistance spot welding: AISI304L/AISI1005,” Pollack Periodica, vol. 20, no. 1, pp. 102–109, 2025, doi: 10.1556/606.2024.01142.

[8] Y. Yang, N. Patil, S. Askar, and A. Kumar, “Machine learning-guided study of residual stress, distortion, and peak temperature in stainless steel laser welding,” Applied Physics A, vol. 131, Art. no. 44, 2025, doi: 10.1007/s00339-024-08145-8.

[9] M. Zhang, Y. Lu, S. Chen, L. Rong, and H. Lu, “Effect of dilution ratio of the first 309L cladding layer on the microstructure and mechanical properties of weld joint of connecting pipe-nozzle to safe-end in nuclear power plant,” Acta Metallurgica Sinica, vol. 56, no. 8, pp. 1057–1066, 2020, doi: 10.11900/0412.1961.2019.00449.

[10] M. A. Valiente Bermejo, D. Eyzop, K. Hurtig, and L. Karlsson, “Welding of large thickness super duplex stainless steel: Microstructure and properties,” Metals, vol. 11, no. 8, Art. no. 1184, 2021, doi: 10.3390/met11081184.

[11] A. Di Schino, “Manufacturing and applications of stainless steels,” Metals, vol. 10, no. 3, Art. no. 327, 2020, doi: 10.3390/met10030327.

[12] F. A. A. Macedo et al., “Influence of the interpass welding temperature on microstructure and corrosion resistance of superduplex stainless steel SAF 2507,” Materials Research, vol. 24, no. 3, 2021, https://doi.org/10.1590/1980-5373-MR-2020-0239.

[13] A. Higelin, S. Le Manchet, G. Passot, et al., “Heat-affected zone ferrite content control of a duplex stainless steel grade to enhance weldability,” Welding in the World, vol. 66, no. 8, pp. 1503–1519, 2022, doi: 10.1007/s40194-022-01326-0.

[14] P. Bellamkonda, M. Dwivedy, M. Sudersanan, et al., “Influence of welding processes on the microstructure and mechanical properties of duplex stainless steel parts fabricated by wire arc additive manufacturing,” Metals and Materials International, vol. 31, pp. 368–391, 2025, doi: 10.1007/s12540-024-01753-2.

[15] A. H. Abbood, M. H. Sir, and N. S. M. Namer, “Corrosion behavior in different media of dissimilar super duplex stainless steel 2507 and austenitic stainless steel 316 welding by using GTAW process with filler type 316L,” Journal of Techniques, vol. 5, no. 3, pp. 185–193, 2023, doi: 10.51173/jt.v5i3.1103.

[16] M. Maslak, M. Stankiewicz, and B. Ślazak, “Duplex steels used in building structures and their resistance to chloride corrosion,” Materials, vol. 14, no. 19, Art. no. 5666, 2021, doi: 10.3390/ma14195666.

[17] A. S. Fedorov and A. I. Zhitenev, “Duplex stainless steels: Requirements, challenges, and solutions,” Metallurgist, vol. 68, pp. 1809–1818, 2025, doi: 10.1007/s11015-025-01894-8.

[18] L. Karlsson, “Welding duplex stainless steels—A review of current recommendations,” Welding in the World, vol. 56, no. 5–6, pp. 65–76, 2012, doi: 10.1007/BF03321351.

[19] B. H. Lee et al., “Intergranular corrosion characteristics of super duplex stainless steel at various interpass temperatures,” International Journal of Electrochemical Science, vol. 10, pp. 7535–7545, 2015, https://doi.org/10.1016/S1452-3981(23)17369-X.

[20] P. Paulraj and R. Garg, “Effect of intermetallic phases on corrosion behavior and mechanical properties of duplex stainless steel and super-duplex stainless steel,” Advances in Science and Technology Research Journal, vol. 9, pp. 87–105, 2015, doi: 10.12913/22998624/59090.

[21] V. D. Cojocaru, M. L. Angelescu, N. Șerban, N. Zărnescu-Ivan, and E. M. Cojocaru, “Effects of solution treatment on the microstructure and mechanical properties of UNS S32750/F53/1.4410 SDSS alloy,” Materials, vol. 18, no. 23, Art. no. 5447, 2025, doi: 10.3390/ma18235447.

[22] C. R. Xavier et al., “An experimental and numerical approach for the welding effects on the duplex stainless steel microstructure,” Materials Research, 2015, https://doi.org/10.1590/1516-1439.302014.

[23] D. Vysochinskiy and D. Rybakov, “On the effect of various heat treatments on microstructure of AISI 4130 steel used in sour service pipes,” in Proceedings of the ASME 2020 39th International Conference on Ocean, Offshore and Arctic Engineering (OMAE2020), vol. 3, Materials Technology, Virtual Conference, Aug. 3–7, 2020, Paper V003T03A008, doi: 10.1115/OMAE2020-18017.

[24] L. Pezzato and I. Calliari, “Advances in duplex stainless steels,” Materials, vol. 15, no. 20, Art. no. 7132, 2022, doi: 10.3390/ma15207132.

[25] J. A. Castro et al., “Effects of local heat input conditions on the thermophysical properties of super duplex stainless steels,” Materials Research, 2018, https://doi.org/10.1590/1980-5373-MR-2017-0384.

[26] H. Sieurin and R. Sandström, “Sigma phase precipitation in duplex stainless steel 2205,” Materials Science and Engineering: A, vol. 444, no. 1–2, pp. 271–276, 2007, https://doi.org/10.1016/j.msea.2006.08.107.

[27] C. Örnek, M. G. Burke, T. Hashimoto, and D. L. Engelberg, “748 K (475 °C) embrittlement of duplex stainless steel: Effect on microstructure and fracture behavior,” Metallurgical and Materials Transactions A, vol. 48, no. 4, pp. 1653–1665, 2017, doi: 10.1007/s11661-016-3944-2.

[28] O. S. Barrak, H. Ben Slama, S. Ben-Elechi, and S. Chatti, “Resistance spot welding of dissimilar metals (AISI 1005 and AISI 304L): Experimental and numerical investigation of tensile-shear and vibration loads,” Journal of Techniques, vol. 7, no. 4, pp. 53–67, 2025, doi: 10.51173/jt.v7i4.2776.

[29] H. Tan, Y. Jiang, B. Deng, T. Sun, J. Xu, and J. Li, “Effect of annealing temperature on the pitting corrosion resistance of super duplex stainless steel UNS S32750,” Materials Characterization, vol. 60, no. 9, pp. 1049–1054, 2009, https://doi.org/10.1016/j.matchar.2009.04.009.

[30] H. Hemmer and Ø. Grong, “A process model for the heat-affected zone microstructure evolution in duplex stainless steel weldments: Part I. The model,” Metallurgical and Materials Transactions A, vol. 30, no. 11, pp. 2915–2929, 1999. https://doi.org/10.1007/s11661-999-0129-2.

[31] P. Ferro and F. Bonollo, “A semiempirical model for sigma-phase precipitation in duplex and superduplex stainless steels,” Metallurgical and Materials Transactions A, vol. 43, pp. 1109–1116, 2012. https://doi.org/10.1007/s11661-011-0966-7.

[32] C. R. Xavier et al., “Numerical prediction for the effects of welding interpass temperature on the thermal history and microstructure of duplex stainless steels,” Materials Research, vol. 26, 2023, https://doi.org/10.1590/1980-5373-MR-2022-0529.

[33] P. Poulain, J. Wang, S. Bouvier, S. Williams, S. Budnyk, and A. Gavrilovic-Wohlmuther, “Impact of interpass temperature on the microstructure and mechanical properties of super duplex stainless steel in CW-GMA additive manufacturing,” Journal of Manufacturing Processes, vol. 146, pp. 30–43, 2025, doi: 10.1016/j.jmapro.2025.04.091.

[34] B. Šimeková et al., “Microstructural and mechanical characterization of the laser beam welded SAF 2507 super-duplex stainless steel,” Metals, vol. 14, no. 10, Art. no. 1184, 2024, doi: 10.3390/met14101184.

[35] P. Kanagaraj, B. Visvalingam, V. Varadhan, and K. Radhakrishnan, “Influence of root pass welding techniques (GTAW and RMD) on metallurgical, mechanical and corrosion behaviour of gas metal arc welded duplex stainless-steel plates,” Canadian Metallurgical Quarterly, pp. 1–27, 2026, doi: 10.1080/00084433.2026.2659551.

[36] T. Tóth, A. C. Hesse, V. Kárpáti et al., “Microstructural and mechanical properties of electron beam welded super duplex stainless steel,” Welding in the World, vol. 68, pp. 1929–1940, 2024, doi: 10.1007/s40194-024-01680-1.

[37] S. Kumar, Y. Kumar, and K. E. K. Vimal, “Microstructural and corrosion behavior of thin sheet of stainless steel-grade super duplex 2507 by gas tungsten arc welding,” SAE International Journal of Materials and Manufacturing, 2024, doi: 10.4271/05-17-02-0011.

[38] R. N. Gunn, Duplex Stainless Steels: Microstructure, Properties and Applications. Cambridge, U.K.: Woodhead Publishing, 1997.

[39] A. H. M. Saeed et al., “Welding tantalum by resistance spot welding with metal plating interlayer,” AIP Conference Proceedings, vol. 3105, 2024, https://doi.org/10.1063/5.0212440.

Downloads

Published

2026-06-15

How to Cite

[1]
“Influence of Interpass Welding Temperature on the Microstructure and Mechanical Properties of Super Duplex Stainless Steel AISI 2507”, DJES, vol. 19, no. 2, pp. 171–180, Jun. 2026, doi: 10.24237/djes.2026.19212.

Similar Articles

81-90 of 350

You may also start an advanced similarity search for this article.